Archives for Chemistry Experiments of (S)-( )-5-Oxo-2-tetrahydrofurancarboxylic Acid

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In homogeneous catalysis, the catalyst is in the same phase as the reactant. The number of collisions between reactants and catalyst is at a maximum.In a patent, 21461-84-7, name is (S)-( )-5-Oxo-2-tetrahydrofurancarboxylic Acid, introducing its new discovery. Recommanded Product: (S)-( )-5-Oxo-2-tetrahydrofurancarboxylic Acid

Diastereoselectivity of 1,3-dipolar cycloaddition reactions of benzyl azide, diazomethane, a nitrile oxide and a nitrile imine to alpha-methylidene-gamma-lactone dipolarophile was effectively controlled by a bulky gamma-substituent, 4-methyl-2,6,7-trioxabicyclo[2.2.2]octan-1-yl in gamma-position of the dipolarophile. The dipoles added from the less hindered face of the double bond with an excellent selectivity. Enantiomerically pure dipolarophile was prepared from the easily available (S)-5-oxotetrahydrohydrofuran-2-carboxylic acid.

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Reference：
Tetrahydrofuran – Wikipedia,
Tetrahydrofuran | (CH2)3CH2O – PubChem