Chemistry is traditionally divided into organic and inorganic chemistry. COA of Formula: C17H16BrClO2, The former is the study of compounds containing at least one carbon-hydrogen bonds.In a patent,Which mentioned a new discovery about 915095-89-5
The invention relates to a method for preparing according to handkerchief row only, in order to 2 – chlorobenzaldehyde as the starting material, after bromo, reduction, halo, and (S)- 3 – phenoxy tetrahydrofuran Friedel-crafts alkylation reaction get intermediate (S)- 3 – (4 – (5 – bromo – 2 – benzylic) phenoxy) tetrahydrofuran, then with 2, 3, 4, 6 – trimethyl silicon-based – D – four – O – glucolactone by condensation, ether, prepared according to handkerchief row only escapes the methoxy hypoglycemic. The advantage of this invention is characterized in that: the invention according to handkerchief row only of the preparation method, compared with the prior synthetic method, in order to 2 – chlorobenzaldehyde as the starting material, the price of raw materials are cheap and easily obtained, the process is easy to realize industrialization, short synthetic route, and easy to operate; and the preparation process in the process, each temperature condition is easy to control, the reaction conversion rate is relatively high, can make the total yield is up to 75% or more; in addition, through the preparation method of the invention, the product is not easy to isomerization, less impurities, can improve the purity of the product, can make the purity of 99% or more. (by machine translation)
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Reference:
Tetrahydrofuran – Wikipedia,
Tetrahydrofuran | (CH2)3CH2O – PubChem