Brief introduction of Tetrahydrofuran-3-carboxylic acid

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A practical large-scale route to an MCH1 receptor antagonist is described. A Staudinger beta-lactam synthesis of an imine and an in situ generated ketene was utilized as a key step for the preparation of a spiro-azetidine building block. The reaction was demonstrated in both batch and flow mode and a comparison of these techniques is described.

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Reference：
Tetrahydrofuran – Wikipedia,
Tetrahydrofuran | (CH2)3CH2O – PubChem