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Synthesis of 4,4?-disubstituted azepines via ring-closing metathesis reaction and asymmetric arylation of lactones

The syntheses of the title compounds were accomplished via an original sequence of reactions including the ring-closing metathesis of omega-dienes by using the second-generation Grubbs’ catalyst. The chiral diene precursors are available in racemic or optically enriched form from the corresponding alpha,alpha?-disubstituted lactones derivatives. Georg Thieme Verlag Stuttgart.

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Reference£º
Tetrahydrofuran – Wikipedia,
Tetrahydrofuran | (CH2)3CH2O – PubChem