453-20-3, 3-Hydroxytetrahydrofuran is a Tetrahydrofurans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated,453-20-3
3-Hydroxytetrahydrofuran (4.4 g, 50 mmol) was dissolved in dichloromethane (50 mL) under ice-cooling,Triethylamine (7.6 g, 75 mmol) was added and stirred for 10 min,Methylsulfonyl chloride (6.3 g, 55 mmol) was slowly added dropwise,After completion of the dropwise addition, the mixture was stirred at room temperature for 1 hour,Washed with saturated aqueous sodium chloride solution (50 mL)The organic phase was concentrated under reduced pressure to give 8.8 g of crude product.
The synthetic route of 453-20-3 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Shandong Xuanzhu Pharma Co., Ltd.; Wu, Yongqian; (38 pag.)CN104788412; (2017); B;,
Tetrahydrofuran – Wikipedia
Tetrahydrofuran | (CH2)3CH2O – PubChem