1679-47-6, 3-Methyldihydrofuran-2(3H)-one is a Tetrahydrofurans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
To alpha-methyl-gamma-butyrolactone (130 g, 1.3 mol) was added phosphoroustribromide (101 mL, 1.13 mol) and this was then heated at reflux for 8 hours. The reaction was slowly poured onto iced water (500 mL). Dichloromethane (500 mL) was added and this was stirred overnight at ambient temperature. The layers were separated, dried over magnesium sulphate, filtered, and evaporated to dryness. The resultant yellow oil was passed through a pad of silica (3:1 hexane:ethyl acetate). This gave 18 (158.5 g, 67%) as an oil., 1679-47-6
The synthetic route of 1679-47-6 has been constantly updated, and we look forward to future research findings.
Reference£º
Article; Wainwright, Philip; Maddaford, Adrian; Zhang, Xiurong; Billington, Helen; Leese, David; Glen, Rebecca; Pryde, David C.; Middleton, Donald S.; Stephenson, Peter T.; Sutton, Scott; Nucleosides, nucleotides and nucleic acids; vol. 32; 9; (2013); p. 477 – 492;,
Tetrahydrofuran – Wikipedia
Tetrahydrofuran | (CH2)3CH2O – PubChem