4100-80-5, 3-Methyldihydrofuran-2,5-dione is a Tetrahydrofurans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
General procedure: A solution of 13 (0.06 mmol) with DMAP (1 equiv) and an appropriate acid anhydride (10 equiv) in anhydrous pyridine(10 ml) was stirred at 155 C for 2 h in a microwave oven (Biotage). The reaction mixture was diluted with EtOAc and neutralized with HCl (1 N) and then extracted with EtOAc. The combined organic layers were washed with brine, dried over MgSO4, and concentrated in vacuum to afford the crude product, followed by chromatographyon a silica gel column and recrystallization to give13e-m.
4100-80-5 3-Methyldihydrofuran-2,5-dione 20051, aTetrahydrofurans compound, is more and more widely used in various.
Reference£º
Article; Wu, Haifeng; Ma, Guoxu; Yang, Qinwen; Zhu, Yindi; Huang, Li; Tian, Yu; Yang, Xiaoming; Zhang, Menghan; Chen, Chin-Ho; Morris-Natschke, Susan L.; Yang, Meihua; Xu, Xudong; Lee, Kuo-Hsiung; European Journal of Medicinal Chemistry; vol. 166; (2019); p. 159 – 166;,
Tetrahydrofuran – Wikipedia
Tetrahydrofuran | (CH2)3CH2O – PubChem